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Beilstein J. Org. Chem. 2008, 4, No. 43, doi:10.3762/bjoc.4.43
Graphical Abstract
Scheme 1: Synthesis of iodides for radical cyclisation. Reagents and conditions: (i) LiC≡CPh, THF, −78 °C to ...
Scheme 2: Radical cyclisation of compounds 7a and 7b.
Scheme 3: Radical cyclisation of compound 9b.
Figure 1: Structures of compounds 18 and 19.
Figure 2: Monte Carlo search on the simplified “trans” structures (structures shown are within 2 kcal/mol).
Figure 3: Monte Carlo search on the simplified “cis” structures (structures shown are within 2 kcal/mol).
Scheme 4: Synthesis of iodides from compounds 6a and 6b. Reagents and conditions: (i) PCC, 4 Å molecular siev...
Scheme 5: Radical cyclisation of compounds 27 and 29. Reagents and conditions: (i) Bu3SnH, AIBN, benzene, 80 ...
Scheme 6: Radical cyclisation of compounds 26 and 28. Reagents and conditions: (i) Bu3SnH, AIBN, benzene, 80 ...
Scheme 7: Synthesis of compounds 55 and 56.